NMR Spectra of Compound X

Figure 1.  Compound X's 1H NMR spectrum.  There is a very broad, weak peak that is very hard to see at around 7 ppm that integrates as 1 hydrogen.

Figure 3.  13C NMR spectrum of compound X.  The peaks near 77 ppm arise from residual CHCl3.

 

10.41 ppm (integration = 1) Click to enlarge. 174.899 ppm 162.426 ppm 137.170 ppm 131.164 ppm 119.812 ppm 118.058 ppm 111.573 ppm Residual undeuterated chloroform