NMR Solvent Properties
| Solvent | d 1H (ppm) | JH-D(Hz) | d 13C (ppm) | JC-D (ppm) | d 1H of HOD (ppm) | Temp. Range (°C) |
|---|---|---|---|---|---|---|
| Acetic Acid | 11.65 (1) | 178.99 (1) | 11.5 | 17 - 118 | ||
| 2.04 (5) | 2.2 | 20.0 (7) | ||||
| Acetone | 2.05 (5) | 2.2 | 206.68 (13) | 0.9 | 2.8 | -94 - 57 |
| 29.2 (7) | 19.4 | |||||
| Acetonitrile | 1.94 (5) | 2.5 | 118.69 (1) | 2.1 | -45 - 82 | |
| 1.39 (7) | 21.0 | |||||
| Benzene | 7.16 (1) | 128.39 (3) | 24.3 | 0.4 | 5 - 80 | |
| Chloroform | 7.27 (1) | 77.23 (3) | 32.0 | 1.5 | -64 - 62 | |
| Cyclohexane | 1.38 (1) | 26.43 (5) | 19.0 | 0.8 | 6 - 81 | |
| Water | 4.80 (DSS) | 4.8 | 3.8 - 101.4 | |||
| 4.81 (TSP) | ||||||
| DMF | 8.03 (1) | 163.15 (5) | 29.4 | 3.5 | -61 - 153 | |
| 2.92 (5) | 1.9 | 34.89 (7) | 21.0 | |||
| 2.75 | 1.9 | 29.76 (7) | 21.1 | |||
| DMSO | 2.50 (5) | 1.9 | 39.51 (7) | 21.0 | 3.3 | 18 - 189 |
| Dioxane | 3.53 (m) | 66.66 (5) | 21.9 | 2.4 | 12 - 101 | |
| Ethanol | 5.29 (1) | 56.96 (5) | 22 | 5.3 | <-130 - 79 | |
| 3.56 (1) | ||||||
| 1.11 (m) | ||||||
| Methanol | 4.87 (1) | 49.15 (7) | 21.4 | 4.9 | -98 - 65 | |
| 3.31 (5) | 1.7 | |||||
| Methylene chloride | 5.32 (3) | 1.1 | 54.00 (5) | 27.2 | 1.5 | -95 - 40 |
| Pyridine | 8.74 (1) | 150.35 (3) | 27.5 | 5.0 | -42 - 116 | |
| 7.58 (1) | 135.91 (3) | 24.5 | ||||
| 7.22 (1) | 123.57 (5) | 25.0 | ||||
| THF | 3.58 (1) | 67.57 (5) | 22.2 | 2.4 - 2.5 | -109 - 66 | |
| 1.73 (1) | 25.37 (1) | 20.2 | ||||
| Toluene | 7.09 (m) | 137.86 (1) | 0.4 | -95 - 111 | ||
| 7.00 (1) | 129.24 (3) | 23.0 | ||||
| 6.58 (5) | 128.33 (3) | 24.0 | ||||
| 20.4 (7) | 10.0 | |||||
| TFA | 11.50 (1) | 164.2 (4) | 11.5 | -15 - 72 | ||
| 116.6 (4) |
From Cambridge Isotope Laboratories NMR Solvent Data Chart, 1994.
Download this file in PDF format.